Effect of Line Filter NH2P-LF (1)
Asahipak
NH2P-50 can be more easily with using a line filter,
NH2P-LF. Figure (b) is a chromatogram after using
NH2P-50 without NH2P-LF for 50 hours, and it is clear that the column performance
has changed compared with the initial chromatogram (figure (a)). The reason of
the change is not the deterioration of the column but the contamination of the
column by extraneous substances such as heavy metals from devece and anions in the eluent. Figure (c) is
a chromatogram after using NH2P-50 with NH2P-LF for 135 hours. We can see that
there is almost no change between (a) and (c). Regarding the way how to connect
NH2P-LF, refer to
Connection of NH2P-LF.
Sample : 0.2% each, 5micro-L
1.
meso-Erythritol
2.
Xylitol
3.
Fructose
4.
Mannose
5.
Glucose
6.
myo-Inositol
7.
Sucrose
8.
Lactose
9.
Maltose
10.
Raffinose
Column : Shodex Asahipak NH2P-50 4E (4.6mmID*250mm)
Eluent : CH3CN/H2O=75/25
Flow rate : 1.0mL/min
Detector : Shodex RI
Column temp. : 25deg-C