Analysis of Oligopeptides with Acidic and Alkaline Eluent
Oligopeptides were analyzed using Asahipak
ODP-50 6D (a column for reversed phase chromatography) with acidic and alkaline eluent.
Please refer to
Effect of Eluent pH (ODP).
Sample :
1.
Glu-Gly-Phe
2.
Met-Enkephalin
3.
Leu-Enkephalin
4.
Leu-Trp-Met
Column : Shodex Asahipak ODP-50 6D (6.0mmID*150mm)
Eluent : (1); 0.05% TFA aq./CH3CN=85/15
(2); 50mM Ammonium acetate(pH10.0)/CH3CN=85/15
Flow rate : 1.0mL/min
Detector : UV(220nm)
Column temp. : 30deg-C