Nucleotides (5)
Nucleotides were analyzed using AXpak
WA-624 (a column for weak anion exchange chromatography).
Sample :
1. 5'
CMP , 2. 5'
TMP
3. 5'
IMP , 4. 5'
AMP
5. 5'
GMP , 6. 3'
GMP
7. 3'
CMP , 8. 5'
UDP
9. 5'
ADP , 10. 5'
CTP
11. 5'
UTP , 12. 5'
ATP
13. 5'
GTP
Column : Shodex AXpak WA-624 (6.0mmID*150mm)
Eluent : (A); 0.1M NaH2PO4 aq./CH3CN=90/10
(B); 0.5M NaH2PO4 aq./CH3CN=80/20
Linear gradient: 0min to30min, (A) to (B)
Flow rate : 1.0mL/min
Detector : UV(260nm)
Column temp. : 60deg-C