Gluconic Acids
The relative hydrophilicity of gluconic acids with similar molecular
structures can be decreased due to their suppressed dissociation in the
acidic eluent. Thus, they are retained in RSpak
DE-613 column by reversed phase mode
and separated.
Sample :
1.
HCl
2.
2-Ketogluconic acid
3.
Gluconic acid
4.
5-Ketogluconic acid
5.
Tartaric acid
6.
Glycolic acid
Column : Shodex RSpak DE-613 (6.0mmID*150mm)
Eluent : 2mM HClO4 aq.
Reagent : 1/10 ST3-R (for post-column method)
Flow rate : (Eluent); 0.5mL/min, (Reagent); 0.2mL/min
Detector : VIS(430nm)
Column temp. : 30 to 32deg-C