Organic Acids in White Wine
Organic acids in white wine were analyzed using RSpak
KC-811.
Fruit contains a large amount of malic acid. For wine, malic acid is transformed
to lactic acid by enzymes during malolactic fermentation. The result of this transformation
is said to give wine a mild taste. For high quality white wine, the chromatogram
shows almost all the malic acid has been transformed to lactic acid.
Sample :
Wine
1.
Citric acid
2.
Tartaric acid
3.
Malic acid
4.
Succinic acid
5.
Lactic acid
6.
Fumaric acid
7.
Acetic acid
8.
Pyroglutamic acid
Columns : Shodex RSpak KC-LG (8.0mmID*50mm) + KC-811 (8.0mmID*300mm) x 2
Eluent : 3mM HClO4 aq.
Reagent : 10-fold diluted ST3-R (for post-column method)
Flow rate : (Eluent); 1.0mL/min, (Reagent); 0.7mL/min
Detector : VIS(430nm)
Column temp. : 45deg-C