Procainamides (1)
Procainamides were analyzed using RSpak
DE-613 (a column
for reversed phase chromatography) with alkaline eluent.
Sample : 8micro-L, 0.1% each
1.
Salicylic acid
2.
Caffeine
3.
N-Acetylprocainamide
4.
Procainamide
Column : Shodex RSpak DE-613 (6.0mmID*150mm)
Eluent : 50mM Na2HPO4(pH9.7)/CH3CN=70/30
Flow rate : 1.0mL/min
Detector : UV(254nm)
Column temp. : 60deg-C