Fatty Acids (4) (RP18-413)
Fatty acids were analyzed using RSpak
RP18-413 (a column
for reversed phase chromatography). Capric acid could be eluted after V
0
with addition of 0.1% H
3PO
4 to eluent.
Sample : C
nH
2n+1COOH, 30micro-L
1.
Capric acid (n=9)
2.
Lauric acid (n=11)
3.
Myristic acid (n=13)
4.
Palmitic acid (n=15)
5.
Stearic acid (n=17)
6.
Arachidic acid, Eicosanoic acid (n=19)
Column : Shodex RSpak RP18-413 (4.6mmID*150mm)
Eluent : 0.1% H3PO4 aq./CH3CN/THF=30/50/20
Flow rate : 0.7mL/min
Detector : Shodex RI
Column temp. : 40deg-C