Comparison of Separation: Linear Type and Column Connection
A compasion of the separation of polystyrene by three linear type columns and
connection of three different columns is shown.
Sample :
1.
PS, Polystyrene (MW: 9,120,000)
2.
PS, Polystyrene (MW: 1,100,000)
3.
PS, Polystyrene (MW: 410,000)
4.
PS, Polystyrene (MW: 128,000)
5.
PS, Polystyrene (MW: 33,000)
6.
PS, Polystyrene (MW: 10,200)
7.
PS, Polystyrene (MW: 1,350)
8.
n-Propylbenzene (MW: 120)
Columns : Shodex GPC KF-806 + KF-805 + KF-803, KF-806L x 3 (8.0mmID*300mm each)
Eluent : THF
Flow rate : 1.0mL/min
Detector : Shodex RI
Column temp. : Room temp.