Effect of Flow Rate (KF-602)
For GPC
KF-602, the relation between HETP (height equivalent
to a theoretical plate) and flow rate is shown here. The value of HETP is almost
the same in the range of 0.4 to 0.8mL/min. However, outside of the range, the
value of HETP is higher. This is true for other grade of Shodex GPC KF-series
columns. When using the columns replacing the in-column solvent from original
solvent (THF) to other solvents, check the pressure not to exceed the maximum
usable pressure because the pressure will be higher if the viscosity of the replaced
solvent is higher.
Generally, the use of KF-series columns in the range of 0.4 to 0.6 mL/min is recommended.
Sample : 0.1%
Dicyclohexyl phthalate, 5micro-L
Column : Shodex GPC KF-602 (6.0mmID*150mm)
Eluent : THF
Detector : UV(254nm)(small cell volume)
Column temp. : 40deg-C