Sample : 1. Lu, Lutetium 2. Yb, Ytterbium 3. Tm, Thulium 4. Er, Erbium 5. Ho, Holmium 6. Y, Yttrium 7. Dy, Dysprosium 8. Tb, Terbium 9. Gd, Gadolinium 10. Eu, Europium 11. Sm, Samarium 12. Nd, Neodymium 13. Pr, Praseodymium 14. Ce, Cerium 15. La, Lanthanum |
Columns : Shodex IC R-G (4.6mmID*10mm) + R-621 (6.0mmID*50mm) Eluent : (A): 0.1M alpha-Hydroxyisobutyric acid(pH4.0,adjusted by NaOH) (B): 1M alpha-Hydroxyisobutyric acid(pH4.0,adjusted by NaOH) Step gradient: 0min to 15min, 100% (A) 15min to 25min, 20% (B) after 25min, 100% (B) Reagent : 0.005(W/V)% Arsenazo III/0.1M Formate(pH3.5) Flow rate : (Eluent); 1.0mL/min, (Reagent); 1.0mL/min Detector : VIS(655nm) Column temp. : 40deg-C