Phenylenediamines
Isomers of Phenylenediamine analyzed using RSpak
JJ-50 4D
(a mutimode column) is shown.
Sample : 100ppm each, 20micro-L
1.
p-Phenylenediamine
2.
m-Phenylenediamine
3.
o-Phenylenediamine
Column : Shodex RSpak JJ-50 4D (4.6mmID*150mm)
Eluent : 25mM CH3COONH4 buffer(pH9.2)/CH3CN=70/30
Flow rate : 0.4mL/min
Detector : UV(254nm)
Column temp. : 30deg-C