Dialkyltin Compounds

Dialkyltin compounds were analyzed using Asahipak GS-310 7E (a multimode column).
GS-310 7E is an old type of GF-310 HQ.


Sample :
e. Dibutyltin
f. Dioctyltin

Column    : Shodex Asahipak GS-310 7E (7.5mmID*250mm)
Eluent    : 0.01M KH2PO4 buffer(pH2.0)/CH3OH=40/60
Reagent   : 0.005% Morin in CH3OH (for post column reaction)
Flow rate : (Eluent); 1.0mL/min, (Reagent); 0.5mL/min
Detector  : Fluorescence(Ex. 420nm, Em. 500nm)

H.Nakajima et al.,BUNSEKI KAGAKU, 36 (1987) 867