Analysis of Irganox 1010 in Cup of Instant Noodles (Styrene Foam) (GPC/MS)

Irganox 1010 in styrene foam cup for instant noodles was analyzed with GPC/MS using KF-402HQ (a semi-micro organic SEC (GPC) column). Only a low molecule weight domain can be poured into a mass spectrometer (MS) by using GPC mode. KF-402HQ can provide the high sensitivity analysis without pretreatment of samples.
Refer to Simultaneous Analysis of Various Additives of Polymer in Polystyrene (GPC/MS).



Sample : 0.1%, 5micro-L
1. Polystyren
2. Irganox 1010

(HPLC)
Instrument   : Agilent 1100
Column       : Shodex GPC KF-402HQ (4.6mmID*250mm) x 2
Eluent       : THF
Flow rate    : 0.3mL/min
Detector     : UV(210nm)
Column temp. : 40deg-C
 
(MS)
Instrument      : Thermo Quest LCQ Advantage
Ionization      : APCI
Capillary temp. : 180deg-C
Vaporizer temp. : 450deg-C
Source voltage  : 6000V
Sheath gas flow : 80L/min